2-Propanol, 2-methyl-, lithium salt (1:1) → HCID 86632376, compound

Participants

Reaction Steps

Using N,N-dimethylformamide solution of ethyl-2-(2-methoxyphenoxy)ethylthiocarbamate 25.5 g (0.1 mol) [J. Chem. Soc., 1952, 2076; J. Chem. Soc., 1952, 2079; Tetrahedron Lett., 1969, 3631], lithium-t-butoxide 1.6 g (0.02 mol) and (S)-2-oxyranylmethoxy-tetrahydropyran 17.38 g (0.11 mol), the procedures as described in Example 1 were carried out to obtain the targeted product.

Provenance & Evidence