HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanol, 2-methyl-, lithium salt (1:1) → HCID 86632379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanol, 2-methyl-, lithium salt (1:1) | HCID 23664764 | — |
| Reactant | HCID 131729415 | HCID 131729415 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86632379 | HCID 86632379 | — |
Reaction Steps
Using N,N-dimethylformamide solution of ethyl-2-(2-methoxyphenoxy)ethylthiocarbamate 51.0 g (0.2 mol), lithium-t-butoxide 3.2 g (0.04 mol) and (R)-2-oxyranylmethoxy-tetrahydropyran 34.76 g (0.22 mol), the procedures as described in Example 1 were carried out to obtain the targeted product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101781B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-d610175d5d9e4615b911e8257f51c1ca |
| Source note | uspto-grants-2012_01 |