HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86632380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 66677026 | HCID 66677026 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86632380 | HCID 86632380 | — |
Reaction Steps
Using dichloromethane solution of the compound of formula 2 prepared in Example 2 80.1 g (0.3 mol), triethylamine 45.5 g (0.45 mol) and methanesulfonyl chloride 37.8 g (0.33 mol), the procedures as described in Example 7 were carried out to obtain the targeted product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101781B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4f42f6dbe522482ea57325f2ab3d6d49 |
| Source note | uspto-grants-2012_01 |