HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → HCID 86632381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 66677026 | HCID 66677026 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86632381 | HCID 86632381 | — |
Reaction Steps
Using dichloromethane solution of the compound of formula 2 prepared in Example 2 42.7 g (0.16 mol), triethylamine 24.3 g (0.24 mol) and p-toluenesulfonyl chloride 33.6 g (0.176 mol), the procedures as described in Example 7 were carried out to obtain the targeted product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101781B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-6fe1c95a3bd3481d8c852f4cdd46897e |
| Source note | uspto-grants-2012_01 |