HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 58807439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | Diethyl p-aminobenzylphosphonate | HCID 88358 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 58807439 | HCID 58807439 | 92% |
Reaction Steps
By the same procedure as described in example 1, diethyl 4-(amino)benzylphosphonate (1.94 g; 8 mmoles), triethylamine (0.87 g; 8.6 mmoles), and methacryloyl chloride (0.9 g; 8.6 mmoles) in toluene (9 ml) afford diethyl 4-(methacrylamido)benzylphosphonate as a slight yellow solid (2.3 g; yield 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08105689B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-54df1c15037d44b594d6465ad395433a |
| Source note | uspto-grants-2012_01 |