HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-5-methylbenzoic acid → 2-Bromo-5-methyl-1-(methoxymethoxymethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-5-methylbenzoic acid | HCID 228080 | — |
| Reactant | 2-Bromo-5-chloro-1-(methoxymethoxymethyl)benzene | HCID 59024677 | — |
| Product | 2-Bromo-5-methyl-1-(methoxymethoxymethyl)benzene | HCID 59008782 | — |
Reaction Steps
This compound was made from 2-bromo-5-methylbenzoic acid in the same manner as compound 18d: 1H NMR (300 MHz, DMSO-d6) δ (ppm) 2.27 (s, 3H), 3.30 (s, 3H), 4.51 (s, 2H), 4.68 (s, 2H), 7.05 (dd, J=7.9, 2.3 Hz, 1H), 7.30 (d, J=1.5 Hz, 1H), 7.46 (d, J=8.2 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106031B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-684cad13069e4bb3983689576aff084b |
| Source note | uspto-grants-2012_01 |