HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6-fluorobenzoic acid → 2-Bromo-6-fluoro-1-(methoxymethoxymethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6-fluorobenzoic acid | HCID 302621 | — |
| Reactant | 2-Bromo-5-chloro-1-(methoxymethoxymethyl)benzene | HCID 59024677 | — |
| Product | 2-Bromo-6-fluoro-1-(methoxymethoxymethyl)benzene | HCID 66704986 | — |
Reaction Steps
This compound was made from 2-bromo-6-fluorobenzoic acid in the same manner as compound 18d: 1H NMR (300 MHz, CDCl3) δ (ppm) 3.43 (s, 3H), 4.74 (s, 2H), 4.76 (d, J=2.1 Hz, 2H), 7.05 (t, J=9.1 Hz, 1H), 7.18 (td, J=8.2, 5.9 Hz, 1H), 7.40 (d, J=8.2 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106031B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4ee919163a0f4208ae4c84976794e4bf |
| Source note | uspto-grants-2012_01 |