HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11265111, compound → HCID 11846121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11265111 | HCID 11265111 | — |
| Reactant | HCID 11845755 | HCID 11845755 | — |
| Product | HCID 11846121 | HCID 11846121 | — |
Reaction Steps
This compound was synthesized from 22a and 7a in a similar manner to compound 9f: colorless oil; 1H NMR (300 MHz, CDCl3) δ (ppm) 3.02 (t, J=6.1 Hz, 2H), 4.34 (t, J=6.1 Hz, 2H), 6.9-7.1 (m, 2H), 7.4-7.6 (m, 3H), 7.8-7.9 (m, 3H); ESI-MS m/z 227 (M+H)+; HPLC purity 95.3%; Anal (C14H12BFO 0.1H2O)C, H.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106031B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-8f20df0452a84cf1bd41fe050bfd0352 |
| Source note | uspto-grants-2012_01 |