HCID 11265111, compound → HCID 11845933, compound

Participants

Reaction Steps

This compound was synthesized from 22b and 7a in a similar manner to compound 9f: colorless oil; 1H NMR (300 MHz, DMSO-d6) δ (ppm) 2.94 (t, J=5.9 Hz, 2H), 4.21 (t, J=5.9 Hz, 2H), 7.28 (t, J=7.9 Hz, 2H), 7.3-7.5 (m, 4H), 7.66 (d, J=7.0 Hz, 1H), 7.75 (d, J=7.6 Hz, 2H); ESI-MS m/z not observed; HPLC purity 96.0%; Anal (C14H13BO) C. H.

Provenance & Evidence