Methylhydrazine → HCID 25128998, compound

HRID 424609Notes

Reaction equation

[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][CH:2]1[O:10][C:11]1[CH:12]=[C:13]([CH:16]=[CH:17][C:18]=1[O:19][CH3:20])C=O.C[O:22][C:23]1C=C([CH:28]=[CH:29][C:30]=1OC)C=O.[CH3:33][NH:34][NH2:35].O.NN>>[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][CH:2]1[O:10][C:11]1[CH:12]=[C:13]([C:29]2[CH:28]=[N:35][N:34]([CH3:33])[C:23](=[O:22])[CH:30]=2)[CH:16]=[CH:17][C:18]=1[O:19][CH3:20]

Participants

Reactant 4

HCID 6061Methylhydrazine

HCID 8419Veratraldehyde

HCID 24654Hydrazine hydrate (1:1)

HCID 157288423-[(2,3-Dihydro-1H-inden-2-yl)oxy]-4-methoxybenzaldehyde

Product 1

HCID 25128998HCID 25128998, compound

Procedure

Using a method similar to Working Example 1 (1)-(4), 3-(2-indanyloxy)-4-methoxybenzaldehyde was substituted for 3,4-dimethoxybenzaldehyde and methylhydrazine for hydrazine hydrate to obtain the title compound.

Sources & evidence

ORD record: ord-22496c5f970c45278d02ba138ddd4534
Source dataset: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08106053B2

Reaction notes

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