Dimethylamine → HCID 66703158, compound

HRID 424619Notes

Reaction equation

HRID 424619 reaction equation
[CH3:1]NC.[CH3:4][NH:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.N[CH:14]([CH:17]1CCC2(OCCO2)[CH2:19][CH2:18]1)[C:15]#[N:16]>>[CH3:4][N:5]([CH3:1])[CH:6]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH:17]1[CH2:18][CH2:19][NH:16][CH2:15][CH2:14]1

Participants

4

Reactant 3

HCID 674DimethylamineHCID 7669N-MethylbenzylamineHCID 66702953HCID 66702953, compound

Product 1

HCID 66703158HCID 66703158, compound

Procedure

Amine units AM 19 and 21 were prepared by the same process using dimethylamine and, respectively, N-methyl(phenyl)methanamine in the preparation of the amino-(1,4-dioxa-spiro[4.5]dec-8-yl)-acetonitrile intermediate.

Workup

  1. customwere prepared by the same process

Sources & evidence

ORD record
ord-24b780dfbf2d4ddaae5577b89a236757
Source dataset
uspto-grants-2012_01
Patent number
US08106055B2

Reaction notes

Loading…