HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-(Dimethylamino)ethane-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-(Dimethylamino)ethanesulfonyl chloride | HCID 14219657 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(Dimethylamino)ethane-1-sulfonamide | HCID 12276893 | — |
Reaction Steps
Ammonia was cautiously added to a cooled solution of the subtitle product of step ii) in THF (50 ml) and stirring maintained until all of the ammonia had evaporated before filtering off the product as a white solid. Yield: 0.88 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106063B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-ffdbe8a39e1749f88ff69dee7676fee7 |
| Source note | uspto-grants-2012_01 |