HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 59212307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 59212543 | HCID 59212543 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 59212307 | HCID 59212307 | — |
Reaction Steps
3-(1,7-Dimethyl-2-oxo-1,2-dihydro-1,6-naphthyridin-3-yl)-4-methylbenzamide 30 (310 mg, 1 mmol) is heated with oxalyl chloride (1 mL) in 1,2-dichloroethane (2 mL) at reflux for 2 h. Solvent is evaporated to give 31 as a white solid which is used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106068B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-ed98fd2868234a68a0688eeaca14c296 |
| Source note | uspto-grants-2012_01 |