Dichloromethane → HCID 57652735, compound

Participants

Reaction Steps

To 2′-bromo-4′-[3-(2,6-dichloro-phenyl)-5-isopropyl-3H-[1,2,3]triazol-4-ylmethoxy]-biphenyl-4-carbonyl chloride (0.043 mmol) in dichloromethane (2 mL) is added s-butyl amine (0.05 mL, 0.5 mmol). The reaction is stirred at room temperature for 1 h and concentrated under reduced pressure. The residue is slurried in 1 N hydrochloric acid, and the solid is filtered to give the title compound (0.011 g). ES/MS m/e 617.0 (M+1).

Provenance & Evidence