HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 66703725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 59786775 | HCID 59786775 | — |
| Product | HCID 66703725 | HCID 66703725 | — |
Reaction Steps
Using general procedure 1 and purification method D with [(1R)-1-{(2R)-oxiran-2-yl}-2-(2,5-difluoro-phenyl)-ethyl]carbamic acid tert-butylester (0.17 g, 0.57 mmol) and methylamine (7 mL, 2M solution in methanol, 14 mmol; used as solvent) gives the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106090B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-d7a7d0ebfc5f4f52bc300b1b08e00a01 |
| Source note | uspto-grants-2012_01 |