Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → Phenol, 3-bromo-, 1-acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 3-Bromophenol | HCID 11563 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Phenol, 3-bromo-, 1-acetate | HCID 141946 | — |
반응 단계
3-bromophenol was dissolved in dichloromethane. Triethylamine (1 eq) and acetic anhydride (2 eq) were added and the mixture was stirred at room temperature for 5 hours. The solvent was eliminated by vacuum evaporation. The evaporation residue was taken up in dichloromethane then dried on magnesium sulfate. The solvent was eliminated by vacuum evaporation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08106097B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-89e702bc6c0441768c9874858355db04 |
| 출처 메모 | uspto-grants-2012_01 |