Allyl glycidyl ether → HCID 131729423, compound

Participants

Reaction Conditions

Reaction Steps

Into a 2.5 liter SUS separable flask equipped with a reflux condenser and a stirrer, 500.0 g of pure water, 399.3 g of iminodiacetic acid (IDA) and 500.0 g of a 48% aqueous solution of sodium hydroxide (hereinafter, abbreviated as 48% NaOH) were charged, and a temperature of the mixture was adjusted to 55° C. while stirring the mixture. Then, 342.4 g of allyl glycidyl ether (AGE) was slowly added dropwise to a reaction system maintained at 55° C. over two hours while stirring. On completion of adding dropwise, the reaction solution was further aged at 55° C. for 1 hour to produce a 50% aqueous solution of AGE-IDA (hereinafter, abbreviated as 50% AGE-IDA).

Provenance & Evidence