HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 672273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Product | HCID 672273 | HCID 672273 | — |
Reaction Steps
A suspension of 1.4 g of powdered KOH in 25 ml of anhydrous acetonitrile stirred under an argon atmosphere was heated to boiling under reflux conditions for 30 minutes and then a solution of 1.15 g of 2-amino-5-chlorobenzophenone in 5 ml of anhydrous acetonitrile was added. The mixture was boiled with a reflux condenser for 12 hours. Cooling was followed by pouring into ice, extraction with ethyl acetate, washing with water and removal of the solvent by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106204B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-7dc9ff98ac3644f5a21d8a9e0abb0b06 |
| Source note | uspto-grants-2012_01 |