Diethylamine → N-Ethyl-9-oxo-9H-xanthene-3-carboxamide

HRID 425276Notes

Reaction equation

HRID 425276 reaction equation
C(NCC)C.[CH2:6]([N:8](CC)[C:9]([C:11]1[CH:12]=[CH:13][C:14]2[C:15](=[O:25])[C:16]3[C:21]([O:22][C:23]=2[CH:24]=1)=[CH:20][CH:19]=[CH:18][CH:17]=3)=[O:10])[CH3:7].C([NH-])C>>[CH2:6]([NH:8][C:9]([C:11]1[CH:12]=[CH:13][C:14]2[C:15](=[O:25])[C:16]3[C:21]([O:22][C:23]=2[CH:24]=1)=[CH:20][CH:19]=[CH:18][CH:17]=3)=[O:10])[CH3:7]

Participants

4

Reactant 3

HCID 8021DiethylamineHCID 187872EthanaminideHCID 15953972N,N-Diethyl-9-oxo-9H-xanthene-3-carboxamide

Product 1

HCID 66702082N-Ethyl-9-oxo-9H-xanthene-3-carboxamide

Procedure

Following Procedure 6, substituting ethylamine for diethylamine, compound 6a was converted into its monoethyl amide. MS m/z (MH+) 267.9.

Sources & evidence

ORD record
ord-0c8431532e9c469e996c5e44dc14ac0d
Source dataset
uspto-grants-2012_01
Patent number
US08106207B2

Reaction notes

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