HRID425961

反应详情

EQUATION

反应方程式

HRID 425961 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Sodium carbonate and 1,4-dibromobutane were added to an acetonitrile solution of 2-{[(1S*,2S*)-2-aminocyclohexyl]amino}-4-chlorobenzonitrile, followed by heating under reflux for 2 days. By post-treating the reaction liquid, 4-chloro-2-{[(1S*,2S*)-2-pyrrolidin-1-ylcyclohexyl]amino}benzonitrile was obtained.

WORKUP

后处理

  1. temperatureby heating
  2. temperatureunder reflux for 2 days
  3. additionBy post-treating
  4. customthe reaction liquid