Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 66703697 | HCID 66703697 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 66703626 | HCID 66703626 | — |
Reaction Steps
4-Chloro-2-[(2,2,6,6-tetramethylpiperidin-4-yl)amino]benzonitrile was dissolved in N-methyl-2-pyrrolidinone, potassium carbonate and iodoethane were added, followed by stirring at 90° C. By post-treating the reaction liquid, 4-chloro-2-[(1-ethyl-2,2,6,6-tetramethylpiperidin-4-yl)amino]benzonitrile was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08106190B2 |
|---|
| Source dataset | uspto-grants-2012_01 |
|---|
| ORD ID | ord-e9783fd8c0ed46cd9c412b4776b86095 |
|---|
| Source note | uspto-grants-2012_01 |
|---|
