HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride → HCID 57867998, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Edukt | 2-(2-hydroxyethylamino)-4-chlorobenzoic Acid | HCID 21251991 | — |
| Edukt | 7-amino-1-methyl-3,4-dihydroquinolin-2(1H)-one | HCID 33699394 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 57867998 | HCID 57867998 | — |
Reaktionsschritte
In dichloromethane, a mixture of 4-chloro-2-[(2-hydroxyethyl)amino]benzoic acid and 7-amino-1-methyl-3,4-dihydroquinolin-2(1H)-one was treated with 1-ethyl-3-[3-(N,N-dimethylamino)propyl]carbodiimide hydrochloride at room temperature to obtain 4-chloro-2-[(2-hydroxyethyl)amino]-N-(1-methyl-2-oxo-1,2,3,4-tetrahydroquinolin-7-yl)benzamide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08106190B2 |
| Quelldatensatz | uspto-grants-2012_01 |
| ORD ID | ord-2ba44da51ec24b71bc756c522d672880 |
| Quellennotiz | uspto-grants-2012_01 |