HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 57614568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 20627849 | HCID 20627849 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57614568 | HCID 57614568 | — |
Reaction Steps
Oxalyl chloride was added to a THF solution of 4-tert-butyl-2-fluorobenzoic acid and stirred for 1 hour, and aqueous ammonia was added to this. By post-treating the reaction liquid, 4-tert-butyl-2-fluorobenzamide was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106190B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-ca5c45644e2b42a3aceae201aee18af3 |
| Source note | uspto-grants-2012_01 |