Triphenylphosphine → HCID 59364377, compound

Participants

Reaction Steps

tert-Butyl 3-(2-azidoethoxy)-3-(5-chloro-2-methylphenyl)propyl(methyl)carbamate (270 mg, 0.707 mmol) was dissolved in THF/H2O (5 mL, 20:1), PPh3 (741 mg, 2.83 mmol) was added in portions. The reaction mixture was stirred at room temperature overnight. The reaction mixture was concentrated in vacuo and used without further purification.

Provenance & Evidence