HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 4496358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 4496358 | HCID 4496358 | 61.5% |
Reaction Steps
A mixture consisting of 34.8 gm (0.37 mol) of phenol, 111 gm (0.81 mol) of potassium carbonate, 89 ml (0.69 mol) of ethyl 2-bromo-propionate and 200 ml of ethanol was boiled for 12 hours, while stirring. Thereafter, the reaction mixture was filtered, and the filtrate was distilled, yielding 44.2 gm of ethyl 2-phenoxy-propionate, b.p. 93°-94° C. at 0.1 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04169720 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-399e58bbba784978be25fe6486206bf2 |
| Source note | uspto-grants-1979_10 |