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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 426438생성일: 2026년 10월 25일

Fenteracol → 2-(2,4,5-Trichloro-phenoxy)-ethyl 2-[4-(4-chlorophenoxymethyl)-phenoxy]-propionate

https://huagongshe.com/reaction/426438

반응식

참여 물질

역할이름HCID투입량
반응물FenteracolHCID 16462—
반응물SodiumHCID 5360545—
반응물Methyl 2-[4-(4-Chlorophenoxy-methyl)-phenoxy]-propionateHCID 19834514—
용매AcetoneHCID 180—
생성물2-(2,4,5-Trichloro-phenoxy)-ethyl 2-[4-(4-chlorophenoxymethyl)-phenoxy]-propionateHCID 53853938—

반응 단계

A mixture consisting of 2.2 gm of methyl 2-[4-(4-chlorophenoxy-methyl)-phenoxy]-propionate, 2.4 gm of 2-(2,4,5-trichloro-phenoxy)-ethanol and 0.03 gm of sodium was heated at about 120°-150° C. and a pressure of 150 mm Hg for four hours. After cooling, the reaction mixture was briefly boiled with acetone, the cooled solution was filtered, and the solvent was removed from the filtrate in vacuo. The residue was recrystallized from ethanol/water, yielding 1.3 gm (36% of theory) of the compound of the formula ##STR19## which had a melting point of 83° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04169720
출처 데이터셋uspto-grants-1979_10
ORD IDord-fac85202ceaa4c29acd8b6831978d813
출처 메모uspto-grants-1979_10