HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4,6-dimethyl pyrimidine → HCID 20390820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4,6-dimethyl pyrimidine | HCID 13021 | — |
| Reactant | Benzenesulfonyl isothiocyanate | HCID 12207092 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20390820 | HCID 20390820 | — |
Reaction Steps
To a dry suspension of 12.4 g of 2-amino-4,-6-dimethypyrimidine in 60 ml of acetonitrile was added 19.9 g of benzenesulfonyl isothiocyanate. The heavy white precipitate which formed was removed by filtration and washed with anhydrous ethyl ether. It melted at 165°170°. The product was N-[(4,6-dimethylpyrimidin-2-yl)-aminothioxomethyl]benzenesulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04169719 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-896d31118cf042299d6807418655dfa4 |
| Source note | uspto-grants-1979_10 |