Lithium Bromide → HCID 20389720, compound

Participants

Reaction Steps

A solution of 988 mg of the crude material prepared in Example XV in 7.5 ml dry acetone was stirred at 25° under argon with 1.80 gm lithium bromide for 18.25 hours at 25°. The acetone was removed in vacuo and water added to the residue. The mixture was extracted with 95:5 hexaneether. The extracts were washed with 10% aqueous sodium thiosulfate and brine, dried over MgSO4, filtered and evaporated in vacuo to afford 737 mg of a yellow oil having the following structure: ##STR39##

Provenance & Evidence