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HRID426734

反应详情

EQUATION

反应方程式

HRID 426734 的结构方程式

REACTANTS

反应物

2
结构：O=C(N=C=S)c1ccccc1
HCID68284

Benzoyl isothiocyanate

C8H5NOS

结构：Nc1cc(-c2ccccc2)nn1-c1ccccc1
HCID199969

Pyrazole, 5-amino-1,3-diphenyl-

C15H13N3

PRODUCTS

生成物

1
结构：NC(=S)Nc1cc(-c2ccccc2)nn1-c1ccccc1
HCID12763850

N-(1,3-Diphenyl-1H-pyrazol-5-yl)thiourea

C16H14N4S

PROCEDURE

实验过程

1,3-Diphenyl-5-amino pyrazole (117.5 g.) and benzoyl isothiocyanate (89.65 g.) were reacted as described in Example IV to give 119.8 g. of product, mp 198°-201° C.

WORKUP

后处理

  1. customto give 119.8 g