HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53690970, compound → HCID 20389867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53690970 | HCID 53690970 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20389867 | HCID 20389867 | — |
Reaction Steps
To a solution of 51.4 g (0.2 mole) of 5-chloro-2-(2-thienylthio)-benzyl alcohol in 400 ml of toluene is added 173.9 g (2.0 mole) of manganese (IV)-oxide, and stirring is maintained at 20°-25° for 25 hours. The precipitate is then filtered off with suction, and the filtrate is concentrated in vacuo to yield 5-chloro-2-(2-thienylthio)-benzaldehyde as yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04171366 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-8dead94e0a3247e3b1dcb351eebc7b3f |
| Source note | uspto-grants-1979_10 |