HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-Methyl-2-phenethyl-4-phenyl-1,2,3,4-tetrahydro-benzo(b)-thieno[3,2-c]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | 3-Methyl-4-phenyl-1,2,3,4-tetrahydro-benzo(b)-thieno[3,2-c]-pyridine | HCID 20388909 | — |
| Solvent | Isopropanol methanol | HCID 21255859 | — |
| Product | 3-Methyl-2-phenethyl-4-phenyl-1,2,3,4-tetrahydro-benzo(b)-thieno[3,2-c]pyridine | HCID 20388901 | — |
Reaction Steps
Phenethyl bromide is condensed with 3-methyl-4-phenyl-1,2,3,4-tetrahydro-benzo(b)thieno[3,2-c]pyridine (Example 2) according to the procedure described in Example 6. Hydrochloride: white crytals, m.p. 210° C. (isopropanol-methanol); Yield : 72%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04172134 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-d5bfeaaab62c4afbb40c271b1eb5066c |
| Source note | uspto-grants-1979_10 |