HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-[2-(2-Naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 12698958 | HCID 12698958 | — |
| Product | 1-[2-(2-Naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride | HCID 12698959 | — |
Reaction Steps
Ethereal hydrogen chloride is added dropwise to a stirred solution of 1.0 g. of 1-[2-(2-naphthyl)-2-(methoxy)ethyl]imidazole in 100 ml. of anhydrous ether until precipitation is complete. The product is filtered off, washed with ether, air dried and recrystallized from ethyl acetate/methanol to yield 1-[2-(2-naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride, m.p. 171.5°-172.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04172141 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-9a4574fbc46e4c97bb3842766b4d06b0 |
| Source note | uspto-grants-1979_10 |