Potassium Carbonate → HCID 12698958, compound

HRID 426950Notes

Reaction equation

HRID 426950 reaction equation
Cl.[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[CH:12]([O:19][CH3:20])[CH2:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1.C(=O)([O-])[O-].[K+].[K+]>ClCCl>[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[CH:12]([O:19][CH3:20])[CH2:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 126989591-[2-(2-Naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride

Product 1

HCID 12698958HCID 12698958, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

1-[2-(2-naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride (800 mg.) in 50 ml. of dichloromethane is shaken with excess dilute potassium carbonate solution until the salt is completely neutralized. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-[2-(2-naphthyl)-2-(methoxy)ethyl]-imidazole.

Workup

  1. customThe organic layer is then separated
  2. washwashed twice with water
  3. dry with materialdried over magnesium sulfate
  4. customevaporated

Sources & evidence

ORD record
ord-99037d6b6ad94f718cce4b2a707f09d1
Source dataset
uspto-grants-1979_10
Patent number
US04172141

Reaction notes

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