Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene → 4-Vinylpyridine styrene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene | HCID 241 | — |
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | Styrene | HCID 7501 | — |
| 반응물 | 2-Vinylpyridine | HCID 7521 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | 4-Vinylpyridine styrene | HCID 12666455 | 20% |
반응 단계
In a 200 ml three necked flask were charged 21 g of 4-vinylpyridine, 21 g of styrene and 0.1 g of azobisisobutyronitrile and 90 ml of benzene. The mixture was polymerized at 80° C. for 6 hrs under a nitrogen atmosphere. The reaction liquid was poured into a large amount of n-hexane to thereby obtain white precipitates. After filtering and drying, a white powder was obtained. The molar fraction of vinylpyridine in the polymer was 0.57 and the yield was 20%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04172180 |
| 출처 데이터셋 | uspto-grants-1979_10 |
| ORD ID | ord-31e2e703769040e5a59f3f08d630c2bc |
| 출처 메모 | uspto-grants-1979_10 |