HRID426966

反应详情

EQUATION

反应方程式

HRID 426966 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In a 200 ml three necked flask were charged 21 g of 4-vinylpyridine, 21 g of styrene and 0.1 g of azobisisobutyronitrile and 90 ml of benzene. The mixture was polymerized at 80° C. for 6 hrs under a nitrogen atmosphere. The reaction liquid was poured into a large amount of n-hexane to thereby obtain white precipitates. After filtering and drying, a white powder was obtained. The molar fraction of vinylpyridine in the polymer was 0.57 and the yield was 20%.

WORKUP

后处理

  1. customThe mixture was polymerized at 80° C. for 6 hrs under a nitrogen atmosphere
  2. customThe reaction liquid
  3. customto thereby obtain white precipitates
  4. filtrationAfter filtering
  5. customdrying
  6. customa white powder was obtained