9-(2-Cyclohexenyl)-2-ethoxy-9H-adenine → 2-n-Hexyloxy-9-cyclohexyl-9H-adenine

Participants

Reaction Steps

The procedure of Example 8 was repeated except that the 9-(2-cyclohexenyl)-2-ethoxy-9H-adenine used therein was replaced by an equivalent weight of 9-(2-cyclohexenyl)-2-n-hexyloxy-9H-adenine. There was produced the title product in 90% yield; m.p. 57°-60° C. IR(neat): 3500, 1635, 1595, 1500, 1465, 1420, 1400 cm-1. UV: λmaxEtOH 253 nm(ε 7200), 270 nm(ε 10900). NMR(CDCl3): 1.5(21H, m), 4.25(2H, t, J=6.5 Hz), 4.40(1H, m), 6.07(2H, s), 7.54(1H, s).

Provenance & Evidence