2,5-Difluoronitrobenzene → HCID 12438962, compound

HRID 427023Notes

Reaction equation

HRID 427023 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([F:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[NH2:12][C:13]1[CH:17]=[CH:16][S:15][C:14]=1[C:18]([O:20][CH3:21])=[O:19]>C1C=CC=CC=1>[F:8][C:5]1[CH:6]=[CH:7][C:2]([NH:12][C:13]2[CH:17]=[CH:16][S:15][C:14]=2[C:18]([O:20][CH3:21])=[O:19])=[C:3]([N+:9]([O-:11])=[O:10])[CH:4]=1

Participants

4

Reactant 2

HCID 677672,5-DifluoronitrobenzeneHCID 89652Methyl 3-amino-2-thiophenecarboxylate

Product 1

HCID 12438962HCID 12438962, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The title compound was prepared using the process of Example 1(a) but with 2,5-difluoronitrobenzene and methyl 3-aminothiophene-2-carboxylate as starting materials, m.p. 172°-175° C. (benzene).

Sources & evidence

ORD record
ord-6d2202071e78414d8be0e7c99af2d2e4
Source dataset
uspto-grants-1979_10
Patent number
US04172831

Reaction notes

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