HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methylhydroxylamine hydrochloride → 3-(4,5-Diphenyl-oxazol-2-yl)-propionaldehyde O-methyl-oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | 3-(4,5-Diphenyl-1,3-oxazol-2-yl)propanal | HCID 13310002 | — |
| Product | 3-(4,5-Diphenyl-oxazol-2-yl)-propionaldehyde O-methyl-oxime | HCID 76800418 | — |
Reaction Steps
The process described in Method A was followed. 3-(4,5-Diphenyl-1,3-oxazol-2-yl)propanal (554 mg, 2.0 mmol, see Pridgen L. N. et al in Tetrahedron Lett., 25(27), 2835 (1984)) and methoxyamine hydrochloride (222 mg, 2.66 mmol) were used to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536210B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-d3f499d80d1d4768a2e6ec084f8a5946 |
| Source note | uspto-grants-2013_09 |