Hydrochloric Acid → HCID 12361802, compound

HRID 427141Notes

Reaction equation

HRID 427141 reaction equation
Cl.Cl.[CH3:3][N:4]([CH3:20])[CH:5]1[CH2:17][C:16]2[C:15]3[C:10](=[C:11]([CH3:19])[CH:12]=[C:13]([CH3:18])[CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1>CCOCC>[CH3:3][N:4]([CH3:20])[CH:5]1[CH2:17][C:16]2[C:15]3[C:10](=[C:11]([CH3:19])[CH:12]=[C:13]([CH3:18])[CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 123618031H-Carbazol-3-amine, 2,3,4,9-tetrahydro-N,N,6,8-tetramethyl-, hydrochloride (1:1)

Product 1

HCID 12361802HCID 12361802, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Following the procedure given in Example 3 and using 9 g. of 4-dimethylaminocyclohexanone and 11 g. of 2,4-dimethylphenylhydrazine hydrochloride there was obtained, after treatment of the free base in ether with ethereal hydrogen chloride, 10.9 g. of 3-(dimethylamino)-6,8-dimethyl-1,2,3,4-tetrahydrocarbazole hydrochloride; m.p. 312°-315° C.

Sources & evidence

ORD record
ord-e29c46534dc64bf98a0c050a09c7a344
Source dataset
uspto-grants-1979_10
Patent number
US04172834

Reaction notes

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