化工社化工社 化学情報印刷レポート · 研究参考用
1,1-Dimethylhydrazine → 2-(4-Methylvaleryl)furan dimethylhydrazone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1-Dimethylhydrazine | HCID 5976 | — |
| 反応物 | 2-(4-Methyl-1-oxopentyl)furan | HCID 95287 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-(4-Methylvaleryl)furan dimethylhydrazone | HCID 53676133 | — |
反応手順
A solution of 2-(4-methylvaleryl)furan (1 mmol) and N,N-dimethylhydrazine (1.5 mmol) in EtOH was heated at reflux for 24 h. Evaporation and distilation give 2-(4-methylvaleryl)furan dimethylhydrazone as a brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06312662B1 |
| 出典データセット | uspto-grants-2001_11 |
| ORD ID | ord-96464513d39146bbbbb224707a5a4154 |
| 出典メモ | uspto-grants-2001_11 |