1,1-Dimethylhydrazine → 2-(4-Methylvaleryl)furan dimethylhydrazone

HRID 427226Notes

Reaction equation

HRID 427226 reaction equation
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)=O.[CH3:13][N:14]([CH3:16])[NH2:15]>CCO>[CH3:13][N:14]([CH3:16])[N:15]=[C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)[CH2:4][CH2:3][CH:2]([CH3:12])[CH3:1]

Participants

4

Reactant 2

HCID 59761,1-DimethylhydrazineHCID 952872-(4-Methyl-1-oxopentyl)furan

Product 1

HCID 536761332-(4-Methylvaleryl)furan dimethylhydrazone

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 2-(4-methylvaleryl)furan (1 mmol) and N,N-dimethylhydrazine (1.5 mmol) in EtOH was heated at reflux for 24 h. Evaporation and distilation give 2-(4-methylvaleryl)furan dimethylhydrazone as a brown oil.

Workup

  1. temperatureat reflux for 24 h
  2. customEvaporation and distilation

Sources & evidence

ORD record
ord-96464513d39146bbbbb224707a5a4154
Source dataset
uspto-grants-2001_11
Patent number
US06312662B1

Reaction notes

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