HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 18356781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 18356786 | HCID 18356786 | — |
| Product | HCID 18356781 | HCID 18356781 | — |
Reaction Steps
A solution of 0.38 g sodium in 50 ml methanol are added to 4.6 g of the compound from example 4 in 75 ml methanol at room temperature. After stirring over night the mixture is evaporated, re-dissolved in dichloro-methane and filtered to give 4.1 g of the title product (m.p. 82-84° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313072B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-7f09debdf4d840fcae70f27483ab3add |
| Source note | uspto-grants-2001_11 |