HRID427511

反应详情

EQUATION

反应方程式

HRID 427511 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 2-isopropyl-6-methylbenzaldehyd (1.75 g, 10.8 mmol) in methanol (15 ml) was added sodium borohydride (0.35 g, 9.5 mmol) and the mixture was stirred 1 h. at room temperature. The solvent was evaporated under reduced pressure and to the residue was added hexane and water. The organic layer was separated and evaporated under reduced pressure to give 1.73 g (98%) of the title compound as an oil.

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure and to the residue
  2. additionwas added hexane and water
  3. customThe organic layer was separated
  4. customevaporated under reduced pressure