HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)benzoic acid → N1-(4-Methoxybenzoyl)-N2-[4-(methylthio)benzoyl]-1,2-benzenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)benzoic acid | HCID 83230 | — |
| Reactant | N-(2-Aminophenyl)-4-methoxybenzamide | HCID 785232 | — |
| Product | N1-(4-Methoxybenzoyl)-N2-[4-(methylthio)benzoyl]-1,2-benzenediamine | HCID 10834358 | 91% |
Reaction Steps
Using the procedure described in Example 55, Part B, N1-(4-methoxybenzoyl)-1,2-benzenediamine (772 mg, 3.19 mmol) was reacted with 4-(methylthio)benzoic acid (772 mg, 4.59 mmol) to yield 1.13 g (91%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313122B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-2ed78d62d2ec4c39a9a05eb0e7ed2c9f |
| Source note | uspto-grants-2001_11 |