HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69361075, compound → HCID 86585768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69361075 | HCID 69361075 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86585768 | HCID 86585768 | 48% |
Reaction Steps
A mixture of N1-(3-benzyloxybenzoyl)-N2-[1-(4-pyridyl)piperidin-4-ylmethoxycarbonyl]-1,2-benzenediamine (75 mg, 0.14 mmol) and 5% palladium-on-carbon (200 mg) in ethanol (4 mL) was placed under an atmosphere of hydrogen (1 atm). After consumption of the starting material, the mixture was filtered through diatomaceous earth and the filtrate concentrated in vacuo yielding 30 mg (48%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313122B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-3e1634e247e841c6bcbcfa62b2d699f9 |
| Source note | uspto-grants-2001_11 |