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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 427702Generated: October 30, 2026

HCID 69361075, compound → HCID 86585768, compound

https://huagongshe.com/reaction/427702

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69361075HCID 69361075—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 86585768HCID 8658576848%

Reaction Steps

A mixture of N1-(3-benzyloxybenzoyl)-N2-[1-(4-pyridyl)piperidin-4-ylmethoxycarbonyl]-1,2-benzenediamine (75 mg, 0.14 mmol) and 5% palladium-on-carbon (200 mg) in ethanol (4 mL) was placed under an atmosphere of hydrogen (1 atm). After consumption of the starting material, the mixture was filtered through diatomaceous earth and the filtrate concentrated in vacuo yielding 30 mg (48%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06313122B1
Source datasetuspto-grants-2001_11
ORD IDord-3e1634e247e841c6bcbcfa62b2d699f9
Source noteuspto-grants-2001_11