HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 131722967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | HCID 86757563 | HCID 86757563 | — |
| Product | HCID 131722967 | HCID 131722967 | 72.2% |
Reaction Steps
Using a similar procedure to that described in Example 48, Part C, N4-(tert-butoxycarbonyl)-N2-[1-(4-pyridyl)piperidin-4-ylmethoxycarbonyl]-1,2,4-benzenetriamine (380 mg, 0.86 mmol) and 4-chlorobenzoyl chloride (0.12 mL, 0.95 mmol) yielded 360 mg (72%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313122B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-4270491fc2874e73938998ce8875b4e2 |
| Source note | uspto-grants-2001_11 |