Isopropanol → HCID 22568988, compound

HRID 427889Notes

Reaction equation

HRID 427889 reaction equation
[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([CH2:11][CH3:12])[CH:3]=1.[CH:13](O)([CH3:15])[CH3:14]>>[CH2:11]([C:4]1[CH:3]=[C:2]([Br:1])[CH:10]=[CH:9][C:5]=1[C:6]([O:8][CH:13]([CH3:15])[CH3:14])=[O:7])[CH3:12]

Participants

3

Reactant 2

HCID 3776IsopropanolHCID 106570054-Bromo-2-ethylbenzoic acid

Product 1

HCID 22568988HCID 22568988, compound

Procedure

Using General Esterification Procedure A; 4-bromo-2-ethyl-benzoic acid (2.25 g, 9.9 mmols) was combined with isopropyl alcohol to give the title compound as a colorless oil after column chromatography (2% EtOAc-hexanes).

Sources & evidence

ORD record
ord-54ae7500fd7d4bcbbc08f8c2bfcaf3c3
Source dataset
uspto-grants-2001_11
Patent number
US06313107B1

Reaction notes

Loading…