HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-buten-1-OL → HCID 54323857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-buten-1-OL | HCID 11173 | — |
| Reactant | N-(3-chlorophenylacetyl)alanine | HCID 15481783 | — |
| Product | HCID 54323857 | HCID 54323857 | — |
Reaction Steps
Following General Procedure C above and using N-(3-chlorophenylacetyl alanine (from Example D above) and 3-methylbut-2-en-1-ol (Aldrich), the title compound can be prepared. The reaction was monitored by tlc on silica gel and purification was by liquid chromatography using 30% EtOAc/hexane as the eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313152B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-5db82e2e084d48ddbca365735267f543 |
| Source note | uspto-grants-2001_11 |