HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-iodosalicylate → HCID 18357889, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-iodosalicylate | HCID 11380407 | — |
| Reactant | HCID 17867292 | HCID 17867292 | — |
| Product | HCID 18357889 | HCID 18357889 | — |
Reaction Steps
In a similar manner to Example 1(d), by reaction of 6.7 g (17.3 mmol) of α-ethynyl-3,5-di-tert-butyl-4-(2-trimethylsilylethoxymethoxy)benzenemethanol with 4.8 g (17.3 mmol) of methyl 2-hydroxy-4-iodobenzoate, 8.5 g (91%) of the expected ester are obtained in the form of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313162B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-c807b75cacb448e282775794a1ba06d5 |
| Source note | uspto-grants-2001_11 |