HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 23708083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | Lithium | HCID 3028194 | — |
| Reactant | HCID 15389071 | HCID 15389071 | — |
| Product | HCID 23708083 | HCID 23708083 | — |
Reaction Steps
In a similar manner to Example 10, by reaction of 200 mg (5.5 mmol) of 2-hydroxy-4-[3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-1-propynyl]benzoic acid with 23 mg (5.5 mmol) of lithium hydroxide hydrate, 150 mg (74%) of the expected lithium salt are obtained, with a melting point of 225-9° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313162B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-60e161cdc24746699584e67dca2d6a35 |
| Source note | uspto-grants-2001_11 |